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Rinse Schlenk flask B with additional dry THF (2.5 ml × 2) and transfer it to Schlenk flask A. 19. Remove the ice/water bath and keep stirring Schlenk flask A for 15 min at ambient temperature. 20.
Thermal hydrosilylation was accomplished by placing the porous Si sample in liquid 1-dodecene (95%, Sigma-Aldrich) in a Schlenk flask, degassing the liquid with three successive freeze–pump ...